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Vol. 122, Issue 11, November 2010, pp.120-127

 

Bullet

Ammonia Gas Sensing Properties of Nanocrystalline Zn1-xCuxFe2O4 Doped with Noble Metal

 

*S. V. JAGTAP, A. V. KADU, N. N. GEDAM and G. N. CHAUDHARI

Nano Technology Research Laboratory, Department of Chemistry,

Shri Shivaji Science College, Amravati 444602, (M.S.) India

E-mail: ashishkadu26@rediffmail.com

 

 

Received: 5 October 2010   /Accepted: 18 November 2010   /Published: 30 November 2010

 

Abstract: The sensors are required basically for monitoring of trace gases in environment. In order to detect, measure and control these gases; one should know the amount and type of gases present in the environment. Among the most toxic and hazardous gases, it is necessary to detect and monitor the ammonia gas because this is enhance in the agricultural sector by the addition of large amounts of NH3 to cultivated farmland in the form of fertilizers. Nanocrystalline spinel type Zn1-xCuxFe2O4 (x=0, 0.2, 0.4 0.6 & 0.8) has been synthesized by sol-gel citrate method. The synthesized powders were characterized by XRD and SEM. The results revealed that the particle size is in the range of 40–45 nm for Cu–Zn ferrite with good crystallinity. The gas sensing properties were studied towards reducing gases like CO, LPG, NH3 and H2S and it is observed that Cu–Zn ferrite shows high response to ammonia gas at relatively lower operating temperature. The Zn0.6Cu0.4Fe2O4 nanomaterial shows better sensitivity towards NH3 gas at an operating temperature 300 0C. Incorporation of Pd improved the sensitivity, selectivity, response time and reduced the operating temperature from 300 0C to 250 0C for NH3 sensor.

 

Keywords: NH3 sensor, Cu–Zn ferrite, Sensitivity, Selectivity, Palladium

 

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