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Vol. 134, Issue 11, November 2011, pp.170-176

 

Bullet

 

Effect of Annealing on the Structural and Optical Properties of Nano Fiber ZnO Films Deposited by Spray Pyrolysis
 

1 M. R. Islam, *1 J. Podder, 2 S. F. U. Farhad and 3 D. K. Saha

1 Department of Physics, Bangladesh University of Engineering & Technology,

Dhaka-1000, Bangladesh, Tel: +880-2-9665613

2 Industrial Physics Division, BCSIR Laboratories, Dhaka-1205, Bangladesh

3 Materials Science Division, Atomic Energy Centre, Dhaka-1000, Bangladesh

*E-mail: jpodder@phy.buet.ac.bd

 

 

Received: 3 May 2011   /Accepted: 21 November 2011   /Published: 29 November 2011

Handbook of Laboaratory Measurements book

 

Abstract: Nano fiber ZnO films have been deposited on to glass substrate at 200 C by a simple spray pyrolysis technique under atmospheric pressure. The effect of annealing temperature on the structural and optical properties of the as grown films has been studied by Scanning Electron Microscopy (SEM) attached with an EDX, powder X-ray diffraction and UV visible spectroscopy. The atomic weight % of Zinc and Oxygen were found to be 49.22 % and 49.62 % respectively. The SEM micrographs show nano fiber structure and uniform deposition on the substrate. Average grain size of ZnO thin film was found in the range of 21 to 27 nm. The lattice constant a and c of ZnO thin film are determined at different annealing temperatures and values are found slightly larger than those of JCPDS data and lower for the sample annealed at 600 C. The lattice parameters a and c decrease with increasing temperature. It reveals that the samples are poly-crystalline and having with low densities. Band gap energy of ZnO was found in the range of 3.33 to 3.17 eV and decreases with the increase of the annealing temperature.

 

Keywords: ZnO, nano fiber, spray pyrolysis, annealing, X-ray diffraction

 

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